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How to Use PCPDFWIN Software for XRD Analysis
PCPDFWIN is a software that allows you to search and match X-ray diffraction (XRD) data with the PDF database, which contains over 900,000 entries of crystal structures from the International Centre for Diffraction Data (ICDD). PCPDFWIN can help you identify unknown phases, refine lattice parameters, calculate interplanar spacings and angles, and display diffraction patterns and crystal structures. In this article, we will show you how to use PCPDFWIN software for XRD analysis.
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Step 1: Install PCPDFWIN software
To use PCPDFWIN software, you need to have a license from ICDD. You can purchase a license online from http://www.icdd.com/ or contact your local distributor. Once you have a license, you can download the software from the same website or use the CD-ROM that comes with your license. To install PCPDFWIN software, follow the instructions on the screen. You will need to enter your license number and password during the installation process.
Step 2: Load your XRD data
PCPDFWIN software can read XRD data in various formats, such as ASCII, Philips, Rigaku, Siemens, and Bruker. To load your XRD data, click on the File menu and select Open. Then, browse to the folder where your XRD data file is located and select it. You can also drag and drop your XRD data file into the PCPDFWIN window. The software will automatically display your XRD pattern in the main window.
Step 3: Search the PDF database
To search the PDF database for matching entries, click on the Search menu and select Search PDF-4+. This will open a new window where you can specify your search criteria, such as chemical formula, elements, space group, cell parameters, peak positions, peak intensities, and peak widths. You can also use advanced options such as subfiles, modifiers, ranges, and filters to narrow down your search results. After setting your search criteria, click on the Start button to begin the search. The software will display a list of matching entries in the lower part of the window.
Step 4: Compare and select the best match
To compare and select the best match for your XRD data, you can use various tools provided by PCPDFWIN software. For example, you can use the Compare tool to overlay your XRD pattern with the diffraction pattern of a selected entry from the PDF database. You can also use the Quality tool to calculate a quality index (Q) that measures how well your XRD pattern matches with the selected entry. The higher the Q value, the better the match. You can also use the Display tool to view the crystal structure and other information of a selected entry from the PDF database. To select an entry as your best match, click on it and then click on the Accept button.
Step 5: Save and print your results
After selecting your best match, you can save and print your results using PCPDFWIN software. To save your results, click on the File menu and select Save As. Then, choose a file name and format for your results. You can save your results as a text file, an HTML file, or a PCPDFWIN file. To print your results, click on the File menu and select Print. Then, choose a printer and print options for your results. You can print your results as a report or as a graph.
PCPDFWIN is a powerful software that can help you perform XRD analysis using the PDF database. By following these steps, you can use PCPDFWIN software to load your XRD data, search the PDF database, compare and select the best match, and save and print your results. PCPDFWIN software can help you identify unknown phases, refine lattice parameters, calculate interplanar spacings and angles, and display diffraction patterns and crystal structures.